Instrumentation

📘 IRP #1 – Introduction to Flow Diagrams & Materials Selection

(Theoretical summary of all pages – including image-only slides – based on )


1️⃣ Course Idea & Structure – Why This Matters 💡

This course is about how to design industrial processes — especially chemical and biotech systems — and how to make them:

  • Technically sound
  • Controllable
  • Economically viable
  • Safe and reliable

Two major pillars:

🔧 A) Instrumentation & Design

  • How to design processes
  • How to choose components and instruments
  • How to make PFDs and P&IDs
  • How to evaluate costs

🎛️ B) Process Control

  • How to control chemical and biotech processes
  • Understanding control loops
  • Learning PID control
  • Implementing in PLC systems

Employers want engineers who understand this whole chain — not just theory, but how real plants work.


2️⃣ Industrial Control Systems ⚙️

Industrial processes never run perfectly on their own. They are constantly affected by:

  • Disturbances
  • Changes in feed composition
  • Temperature variations
  • Pressure fluctuations

To keep the system stable, we use control loops.


🔁 The Control Loop – Core Concept

A basic control loop consists of:

  • Setpoint (SP) → Desired value
  • Process Variable (PV) → Measured value
  • Sensor + Transmitter → Measures PV
  • Controller → Compares SP and PV
  • Control element (valve/pump) → Adjusts process
  • Feedback loop

The controller calculates an error:

e = SP - PV

It then adjusts the manipulated variable (u).


🎛️ PID Control

PID =

  • P → Proportional
  • I → Integral
  • D → Derivative

⚠️ Important: PID ≠ P&ID

  • PID → Control algorithm
  • P&ID → Diagram

PID control is often implemented in PLCs (Programmable Logic Controllers).


3️⃣ Where Is Process Control Used? 🌍

Practically everywhere:

🧪 pH Control

  • Fermentation
  • Coagulation

🌡 Temperature Control

  • Cooking
  • Brewing
  • Pasteurization

💨 Pressure Control

  • Filtration
  • Water distribution

📏 Level Control

  • Tanks
  • Reactors

Control systems are fundamental in biotech and chemical engineering.


4️⃣ The Exam Structure 🎓

  • Mini project (design + control)
  • Group defense
  • Pass/fail grading

The theoretical goal: Understand how to design and control a process from scratch.


5️⃣ The Design Process 🏗

Design is systematic:

  1. Problem statement
  2. Planning
  3. Implementation
  4. Financial evaluation

Engineering is not just calculations — it includes economics.


6️⃣ Process Flow Diagrams (PFD) 🗺

A PFD shows:

  • Major equipment
  • Process flow
  • Basic connections

It does NOT show:

  • Instrumentation details
  • Control logic

It’s an overview.


📊 PFD with Mass Balances

A more detailed PFD includes:

  • Flow rates
  • Compositions
  • Material balances

This links chemical engineering theory with process design.


7️⃣ P&ID – Process & Instrumentation Diagram 🔍

A P&ID is much more detailed than a PFD.

It includes:

  • Sensors
  • Transmitters
  • Controllers
  • Valves
  • Pumps
  • Signal lines

It shows how control loops are physically implemented.

This is what plant operators and engineers actually use.


8️⃣ ISA 5.1 Instrument Nomenclature 🏷

Standard naming system.

First letter = measured variable:

LetterMeaning
TTemperature
PPressure
LLevel
FFlow

Following letters = function:

LetterMeaning
IIndicator
RRecorder
CController
TTransmitter
VValve
SSwitch
YCompute
AHHigh alarm
ALLow alarm

Example:

PIC = Pressure Indicator Controller

This standardization is critical in industry.


9️⃣ Control Valves (Image Slide Explained) 🚪

Different valve types:

  • Globe valves
  • Diaphragm valves
  • Three-way valves

Valves regulate flow — they are final control elements.


🛑 Valve Failure Modes

Important safety concept:

  • Fail open
  • Fail closed
  • Fail locked
  • Failure mode indeterminate

Failure position depends on safety requirements.

Example:

  • Cooling water valve → often fail open
  • Fuel supply → fail closed

🔌 Signal Types in P&ID

Electric analog:

4–20 mA (industry standard)

Pneumatic:

Instrument air (older systems, explosive areas)

Binary:

On/off (solenoids)

Internal digital communication

Modern plants mainly use electric signals.

Instrument lines are drawn lighter than process lines.


🖥 Instrument Location Symbols

Symbols indicate:

  • Field mounted
  • Local panel mounted
  • Control room mounted
  • PLC / Distributed control system

This tells you where the instrument physically resides.


🔁 Example: Flow Control

Two ways to control flow:

1️⃣ Valve after pump 2️⃣ Variable pump speed

Valve control = cheaper Pump speed control = more energy efficient

Design is always a trade-off between CAPEX and OPEX.


🔬 Unit Operations

Core building blocks of process plants:

  • Distillation
  • Gas–gas operations
  • Liquid–liquid separation
  • Liquid–solid operations
  • Reactors
  • Heat exchangers
  • Gas & liquid handling
  • Solid transport

Understanding these helps you interpret PFDs.


🧪 Tank with pH Control (Design Exercise)

Continuous Stirred Tank Reactor (CSTR):

Requirements:

  • Maintain constant pH
  • Maintain constant level
  • Maintain retention time

So you need:

  • pH sensor + transmitter
  • pH controller
  • Acid dosing pump/valve
  • Level sensor
  • Level controller
  • Possibly flow control

Everything must communicate via signals.

This integrates:

  • Process design
  • Instrumentation
  • Control theory

🧱 Materials Selection

Critical engineering decision.

Must consider:

Operating conditions:

  • Temperature
  • pH
  • Salts
  • Erosion

Fabrication:

  • Welding
  • Casting
  • Machining

Corrosion resistance

Use chemical resistance charts.

Wrong material = failure.


💰 Design Case: Batch vs Continuous Fermentation

You must:

  • Design system
  • Select materials
  • Scale up
  • Estimate CAPEX
  • Estimate OPEX

This links engineering to business reality.


🎓 Mini Project

Apply everything to your own case.

You design:

  • Process
  • Control strategy
  • Equipment
  • Materials
  • Economics

Then defend it.

This simulates real engineering practice.


🧠 Big Picture Takeaways

This lecture establishes:

  • How processes are structured
  • How control loops work
  • How diagrams represent reality
  • Why standardization (ISA) matters
  • Why material selection is critical
  • Why economics cannot be ignored

It connects: Chemical engineering + Instrumentation + Control theory + Economics.

Quiz

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